论文标题
用于控制温度和氦气压力下相对长度变化的高级技术
Advanced technique for measuring relative length changes under control of temperature and helium-gas pressure
论文作者
论文摘要
我们报告了在控制温度($ t $)和氦气压力($ p $)下,用于测量相对长度的高级技术的实现。该系统是Manna等人Rev. Sci中描述的设备的扩展。乐器。 83,085111(2012)由两个$^4 $ HE-浴冷冻剂组成,每个冷冻仪都容纳了压力单元和一个电容式扩散表。压力电池的互连(可以单独控制的温度)打开各种操作模式,以在温度和压力的变化下执行$Δl/l $的测量。该设备的特殊特征包括(1)增加对超过外部压力储层的压力的可能性(1),(2)在温度扫描期间大大提高压力稳定性,(3)以启用持续的压力随着压力降低和增加压力,以及(4)同时测量载有载台的介电常数,中等载中型载媒体,培养基媒介物介质的载体和培养基。 $ \ VAREPSILON _ {\ MATHRM {r}}}^{\ MATHRM {HE}}(T,P)$,沿着相同的$ t $ - $ P $ traightory,用于服用$Δl(t,p)/l $数据。设置的性能通过相对长度变化的测量$(Δl/l)_t $ at $ t = 180 \,\ Mathrm {k} $的单晶NaCl的范围不断变化$ 6 \ \ 6 \,\ m m iq {mpa} \ leq p \ leq p \ leq 40 \ \ \ \ \ \ \,
We report the realization of an advanced technique for measuring relative length changes $ΔL/L$ of mm-sized samples under control of temperature ($T$) and helium-gas pressure ($P$). The system, which is an extension of the apparatus described in Manna et al., Rev. Sci. Instrum. 83, 085111 (2012), consists of two $^4$He-bath cryostats each of which houses a pressure cell and a capacitive dilatometer. The interconnection of the pressure cells, the temperature of which can be controlled individually, opens up various modes of operation to perform measurements of $ΔL/L$ under variation of temperature and pressure. Special features of this apparatus include the possibilities (1) to increase the pressure to values much in excess of the external pressure reservoir, (2) to substantially improve the pressure stability during temperature sweeps, (3) to enable continuous pressure sweeps both with decreasing and increasing pressure, and (4) to simultaneously measure the dielectric constant of the pressure-transmitting medium helium, $\varepsilon_{\mathrm{r}}^{\mathrm{He}}(T,P)$, along the same $T$-$P$ trajectory as used for taking the $ΔL(T,P)/L$ data. The performance of the setup is demonstrated by measurements of relative length changes $(ΔL/L)_T$ at $T=180\,\mathrm{K}$ of single crystalline NaCl upon continuously varying the pressure in the range $6\,\mathrm{MPa}\leq P \leq 40\,\mathrm{MPa}$.